技術文章
Technical articles分析專用色譜儀是(shi)(shi)要進行檢(jian)定(ding)的(de)(de)設備,檢(jian)定(ding)周期一(yi)(yi)般為兩(liang)年一(yi)(yi)次。檢(jian)定(ding)周期到后,可(ke)按新規程(cheng)進行了檢(jian)定(ding),下面譜析工(gong)程(cheng)師(shi)分享(xiang)一(yi)(yi)下檢(jian)定(ding)過(guo)程(cheng)。一(yi)(yi)、新舊規程(cheng)對比新規程(cheng)相對舊規程(cheng)相比,有(you)一(yi)(yi)些變(bian)化,FPD的(de)(de)基(ji)線噪聲(sheng)(sheng)與(yu)漂(piao)移(yi)都是(shi)(shi)0.5nA,允許的(de)(de)基(ji)線漂(piao)移(yi)范(fan)圍大(da)了。ECD以Hz為輸(shu)出信號的(de)(de)噪聲(sheng)(sheng)和漂(piao)移(yi),不用再換算,用起(qi)來很直(zhi)觀。ECD檢(jian)測(ce)器溫(wen)度由原來的(de)(de)230℃改為250℃,是(shi)(shi)大(da)家常用的(de)(de)檢(jian)測(ce)器溫(wen)度。檢(jian)測(ce)限(xian)檢(jian)定(ding)時進樣次數和載氣流速測(ce)量次數由原來的(de)(de)6次改為7次,可(ke)能與(yu)統計概率(lv)有(you)關。二、準備工(gong)作(zuo)檢(jian)定(ding)前(qian),操(cao)作(zuo)人員(yuan)需...
色(se)(se)(se)譜分(fen)(fen)析(xi)(xi)儀主要(yao)是對天(tian)然氣(qi)(qi)含(han)(han)有(you)(you)的(de)(de)(de)不同(tong)成(cheng)分(fen)(fen)的(de)(de)(de)特征信(xin)息進(jin)行檢測(ce),從而得到準確的(de)(de)(de)天(tian)然氣(qi)(qi)成(cheng)分(fen)(fen)含(han)(han)量。色(se)(se)(se)譜分(fen)(fen)析(xi)(xi)儀在(zai)(zai)(zai)實際應用中(zhong),會(hui)進(jin)行多次的(de)(de)(de)吸附、解附等操作(zuo),對出現(xian)色(se)(se)(se)譜的(de)(de)(de)時間進(jin)行分(fen)(fen)析(xi)(xi),并將所含(han)(han)有(you)(you)的(de)(de)(de)成(cheng)分(fen)(fen)含(han)(han)量記錄到后臺系統中(zhong),滿(man)足對天(tian)然氣(qi)(qi)成(cheng)分(fen)(fen)檢測(ce)的(de)(de)(de)需(xu)求(qiu)。色(se)(se)(se)譜分(fen)(fen)析(xi)(xi)儀常見故(gu)障原(yuan)(yuan)因(yin)分(fen)(fen)析(xi)(xi)及處(chu)理措(cuo)施(1)氣(qi)(qi)路污(wu)染。色(se)(se)(se)譜分(fen)(fen)析(xi)(xi)儀在(zai)(zai)(zai)日常工作(zuo)中(zhong),易出現(xian)氣(qi)(qi)路污(wu)染的(de)(de)(de)故(gu)障,主要(yao)的(de)(de)(de)原(yuan)(yuan)因(yin)為天(tian)然氣(qi)(qi)中(zhong)含(han)(han)有(you)(you)濃(nong)度較高的(de)(de)(de)雜質氣(qi)(qi)體(ti)(ti),能通過圖譜中(zhong)直觀觀察雜質氣(qi)(qi)體(ti)(ti)的(de)(de)(de)含(han)(han)量。導致天(tian)然氣(qi)(qi)含(han)(han)有(you)(you)雜質氣(qi)(qi)體(ti)(ti)的(de)(de)(de)主要(yao)原(yuan)(yuan)因(yin)有(you)(you):在(zai)(zai)(zai)色(se)(se)(se)譜分(fen)(fen)析(xi)(xi)儀檢測(ce)管道的(de)(de)(de)進(jin)出口被污(wu)...
1.進樣(yang)(yang)(yang)(yang)(yang)(yang)將(jiang)試樣(yang)(yang)(yang)(yang)(yang)(yang)瓶和(he)(he)氣(qi)相色譜儀進樣(yang)(yang)(yang)(yang)(yang)(yang)口(kou)之間用不銹鋼管或聚四氟乙(yi)(yi)烯管連(lian)接,打開試樣(yang)(yang)(yang)(yang)(yang)(yang)瓶的(de)(de)(de)出口(kou)閥,用氣(qi)樣(yang)(yang)(yang)(yang)(yang)(yang)吹(chui)掃包括(kuo)定(ding)量(liang)管在(zai)內的(de)(de)(de)進樣(yang)(yang)(yang)(yang)(yang)(yang)系統,定(ding)量(liang)管的(de)(de)(de)進樣(yang)(yang)(yang)(yang)(yang)(yang)壓力應(ying)接近大氣(qi)壓力,關閉試樣(yang)(yang)(yang)(yang)(yang)(yang)瓶閥,立即(ji)切(qie)換六(liu)通閥,將(jiang)氣(qi)樣(yang)(yang)(yang)(yang)(yang)(yang)導(dao)入GC。或用真(zhen)(zhen)空法進樣(yang)(yang)(yang)(yang)(yang)(yang)。將(jiang)進樣(yang)(yang)(yang)(yang)(yang)(yang)系統抽(chou)真(zhen)(zhen)空,使(shi)壓力低于(yu)100Pa,將(jiang)與真(zhen)(zhen)空系統連(lian)接的(de)(de)(de)閥關閉,然后仔細地將(jiang)氣(qi)樣(yang)(yang)(yang)(yang)(yang)(yang)從試樣(yang)(yang)(yang)(yang)(yang)(yang)瓶充入定(ding)量(liang)管至所要求的(de)(de)(de)壓力,隨后切(qie)換將(jiang)樣(yang)(yang)(yang)(yang)(yang)(yang)導(dao)入GC。2.分(fen)離乙(yi)(yi)烷和(he)(he)更重組分(fen)、二氧化(hua)碳的(de)(de)(de)分(fen)配柱操作使(shi)用氦氣(qi)或氫氣(qi)作為(wei)載氣(qi),進樣(yang)(yang)(yang)(yang)(yang)(yang),并在(zai)適(shi)當的(de)(de)(de)時候(hou)反吹(chui)重組分(fen),得到(dao)譜圖(tu)。按同樣(yang)(yang)(yang)(yang)(yang)(yang)的(de)(de)(de)方法獲(huo)...
通常,我們用化工氣相色譜(pu)(pu)儀(yi)做試驗時不(bu)出(chu)峰原因是(shi)(shi)(shi)(shi)有(you)很多的(de),而首先(xian)(xian)要(yao)看檢(jian)(jian)(jian)(jian)測什么樣(yang)(yang)品,選擇被(bei)檢(jian)(jian)(jian)(jian)測樣(yang)(yang)品所(suo)用的(de)檢(jian)(jian)(jian)(jian)測器和合適(shi)的(de)色譜(pu)(pu)柱(zhu),就是(shi)(shi)(shi)(shi)檢(jian)(jian)(jian)(jian)測條件(jian)要(yao)合適(shi),還(huan)有(you)柱(zhu)子(zi)(zi)連接的(de)位(wei)置,這些條件(jian)都可(ke)(ke)能造(zao)成(cheng)不(bu)出(chu)峰。一、樣(yang)(yang)品問(wen)題1.樣(yang)(yang)品在氫火焰檢(jian)(jian)(jian)(jian)測器是(shi)(shi)(shi)(shi)否有(you)響應;2.樣(yang)(yang)品是(shi)(shi)(shi)(shi)否與色譜(pu)(pu)柱(zhu)不(bu)匹配;3.樣(yang)(yang)品濃度是(shi)(shi)(shi)(shi)否過低(di),低(di)于(yu)檢(jian)(jian)(jian)(jian)測器檢(jian)(jian)(jian)(jian)出(chu)限;二、化工氣相色譜(pu)(pu)儀(yi)問(wen)題首先(xian)(xian)要(yao)看檢(jian)(jian)(jian)(jian)測什么樣(yang)(yang)品,選擇被(bei)檢(jian)(jian)(jian)(jian)測樣(yang)(yang)品所(suo)用的(de)檢(jian)(jian)(jian)(jian)測器和合適(shi)的(de)色譜(pu)(pu)柱(zhu),再就是(shi)(shi)(shi)(shi)檢(jian)(jian)(jian)(jian)測條件(jian)要(yao)合適(shi).還(huan)有(you)柱(zhu)子(zi)(zi)連接的(de)位(wei)置,這些條件(jian)都可(ke)(ke)能造(zao)成(cheng)不(bu)出(chu)峰。1.載氣:是(shi)(shi)(shi)(shi)否有(you)載氣進入(ru)...
油色(se)(se)(se)譜(pu)分析儀是一(yi)種多(duo)組(zu)份(fen)混(hun)合物的(de)(de)分離與檢測的(de)(de)分析工具。它是以氣(qi)體為流動(dong)相(xiang)(xiang),采用沖洗法的(de)(de)柱色(se)(se)(se)譜(pu)技術。從(cong)結構上看,又是一(yi)個載(zai)氣(qi)連續運行的(de)(de)自動(dong)記錄儀器(qi)。氣(qi)相(xiang)(xiang)色(se)(se)(se)譜(pu)分離是利(li)用試(shi)樣中(zhong)各(ge)組(zu)份(fen)在色(se)(se)(se)譜(pu)柱中(zhong)的(de)(de)氣(qi)相(xiang)(xiang)和固(gu)(gu)定(ding)液液相(xiang)(xiang)間(jian)的(de)(de)分配系(xi)數不同,當(dang)汽化后的(de)(de)試(shi)樣被載(zai)氣(qi)帶入色(se)(se)(se)譜(pu)柱中(zhong)運行時(shi),組(zu)份(fen)就(jiu)(jiu)在其(qi)中(zhong)的(de)(de)兩(liang)相(xiang)(xiang)間(jian)進行反復多(duo)次的(de)(de)分配(吸(xi)附-脫附或溶解-釋(shi)放(fang)),由(you)于固(gu)(gu)定(ding)相(xiang)(xiang)對各(ge)組(zu)份(fen)的(de)(de)吸(xi)附或溶解能力不同(即保(bao)留作用不同),因此(ci)各(ge)組(zu)份(fen)在色(se)(se)(se)譜(pu)柱中(zhong)的(de)(de)運行速(su)度就(jiu)(jiu)不同,經過一(yi)定(ding)的(de)(de)柱長后,便彼此(ci)分離,順序離開色(se)(se)(se)譜(pu)柱進入檢測器(qi),...
高(gao)純度氫(qing)氣(qi)(qi)發生(sheng)(sheng)器(qi)可(ke)(ke)為(wei)國產(chan)、進口氣(qi)(qi)相色譜提供穩定的(de)(de)氫(qing)氣(qi)(qi)氣(qi)(qi)源,操作簡單(dan),只需發動(dong)電源開(kai)(kai)(kai)關,即可(ke)(ke)產(chan)氣(qi)(qi),輸(shu)出壓力穩定,流(liu)量由LED數碼顯現(xian),更直觀醒目。氫(qing)氣(qi)(qi)發生(sheng)(sheng)器(qi)日常使(shi)用(yong)只需補充蒸餾水,氫(qing)氣(qi)(qi)發生(sheng)(sheng)器(qi)可(ke)(ke)連續(xu)使(shi)用(yong),也可(ke)(ke)間斷使(shi)用(yong)。儲液、電解制氫(qing)、排氧一體(ti)化,氫(qing)氣(qi)(qi)發生(sheng)(sheng)器(qi)池(chi)溫(wen)低,壽命持久。氫(qing)氣(qi)(qi)作為(wei)一種綠色動(dong)力介質,可(ke)(ke)同(tong)時滿(man)足(zu)資源、環境(jing)和(he)可(ke)(ke)持續(xu)發展的(de)(de)要求,是其他燃氣(qi)(qi)所不能(neng)比擬的(de)(de)。氫(qing)氣(qi)(qi)發生(sheng)(sheng)器(qi)用(yong)氫(qing)氧火(huo)焰(yan)切開(kai)(kai)(kai),以(yi)替(ti)代傳統連鑄(zhu)坯切開(kai)(kai)(kai)技能(neng),氫(qing)氣(qi)(qi)發生(sheng)(sheng)器(qi)另外在運用(yong)氫(qing)氧火(huo)焰(yan)對原(yuan)設(she)備進行簡易改(gai)造(zao),投入較少。高(gao)純度氫(qing)...
影響高純度(du)氮氣(qi)(qi)發生器(qi)價格的因素很多(duo),因此您可(ke)(ke)以多(duo)找幾家(jia)公司進行(xing)對比(bi)。可(ke)(ke)以試著了解一下。高純度(du)氮氣(qi)(qi)發生器(qi)是一套(tao)能(neng)提取(qu)氮氣(qi)(qi)的設備(bei)(bei),它(ta)主要(yao)應(ying)用(yong)領域為:航空航天(tian)、核(he)電核(he)能(neng)、食(shi)品醫藥、石油(you)化工(gong)、電子工(gong)業、材料工(gong)業和科學(xue)實驗等。上海氣(qi)(qi)譜儀(yi)器(qi)設備(bei)(bei)有(you)限公司從事(shi)高純度(du)氮氣(qi)(qi)發生器(qi)行(xing)業多(duo)年(nian),公司擁有(you)多(duo)種(zhong)類型(xing)(xing)的高純度(du)氮氣(qi)(qi)發生器(qi)可(ke)(ke)供客戶選擇,我(wo)們(men)擁有(you)多(duo)種(zhong)高純度(du)氮氣(qi)(qi)發生器(qi)型(xing)(xing)號,儀(yi)器(qi)性(xing)能(neng)穩(wen)定,*可(ke)(ke)以滿足(zu)進口和國產(chan)氣(qi)(qi)相色譜儀(yi)的配套(tao)使用(yong)。如果您有(you)需(xu)求,歡迎(ying)您的垂詢!高純度(du)氮氣(qi)(qi)發生器(qi)具有(you)工(gong)藝(yi)流程簡(jian)單、自動化程度(du)...
色(se)(se)譜(pu)分析儀(yi)是應用(yong)(yong)色(se)(se)譜(pu)法對物質進(jin)行定(ding)性(xing)(xing)、定(ding)量(liang)分析,及研(yan)究物質的(de)(de)物理、化(hua)學(xue)特(te)性(xing)(xing)的(de)(de)儀(yi)器(qi)。包(bao)括進(jin)樣系統(tong)(tong)、檢測系統(tong)(tong)、記錄和數據(ju)處(chu)理系統(tong)(tong)、溫控(kong)系統(tong)(tong)以(yi)及流動(dong)(dong)相(xiang)控(kong)制(zhi)系統(tong)(tong)等。現(xian)代(dai)的(de)(de)色(se)(se)譜(pu)儀(yi)具有(you)穩定(ding)性(xing)(xing)、靈敏性(xing)(xing)、多用(yong)(yong)性(xing)(xing)和自動(dong)(dong)化(hua)程度高(gao)等特(te)點。有(you)氣(qi)(qi)相(xiang)色(se)(se)譜(pu)儀(yi)、液相(xiang)色(se)(se)譜(pu)儀(yi)和凝膠色(se)(se)譜(pu)儀(yi)等。這些色(se)(se)譜(pu)儀(yi)廣泛地用(yong)(yong)于化(hua)學(xue)產品,高(gao)分子(zi)(zi)材(cai)料的(de)(de)某種含量(liang)的(de)(de)分析,凝膠色(se)(se)譜(pu)還可以(yi)測定(ding)高(gao)分子(zi)(zi)材(cai)料的(de)(de)分子(zi)(zi)量(liang)及其(qi)分布。1、流動(dong)(dong)相(xiang)不同:HPLC為液體(ti)流動(dong)(dong)相(xiang),GC為久性(xing)(xing)氣(qi)(qi)體(ti)作流動(dong)(dong)相(xiang)(通常叫做載氣(qi)(qi))二、進(jin)樣器(qi)不同:高(gao)效液相(xiang)為平頭(tou)進(jin)樣針,氣(qi)(qi)相(xiang)色(se)(se)...